The facility has a number of in-situ testing apparatus that are designed to be placed inside the X-ray CT scanners and enable “in-situ” time-lapse scanning of processes such as deformation, fluid flow, and temperature changes. The testing stages are stored in our dedicated “rig room”, where they can be used outside of the X-ray CT instruments to prepare for beamtime or for standalone testing.

200 N Bose-Deben Fatigue Rig

Key Features

  • Purpose built X-ray CT tension-compression in-situ fatigue rig
  • Peak force: +/- 200 N
  • Static force (continuous): 2.1 kN.
  • Max frequency: 100 Hz
  • Able to perform different waveforms via remote system control.
  • Data acquisition for force and displacement over time.
  • Limited angle X-ray CT data collection.
  • Waveform, amplitude and phase compensation functions.
  • Compatible with the Nikon 320 kV, The High Flux Bay, ZEISS Versa 520 systems and synchrotron beamlines

Fatigue Testing 3 kN Bose-Deben Rig

Key Features

  • Purpose built X-ray CT tension-compression in-situ fatigue rig.
  • Peak force +/- 3 kN.
  • Static force +/- 2.1 kN.
  • Max frequency 100 Hz.
  • Able to perform different waveforms via remote system control.
  • Waveform, amplitude and phase compensation function.
  • Data acquisition for force displacement overtime.
  • Limited angle X-ray CT data collection with 25 mm range of displacement.
  • Compatible with Nikon 320 kV and The High Flux bay at the HMXIF and also synchrotron beamlines

Compression / Tension 2-25 kN Deben Rig

Key Features

  • Specimen diameters ranging from 1 mm – 30 mm.
  • Specimen length between 5 mm – 80 mm.
  • Load cells ranging from 1.25, 2.5, 10 to 25 kN with alternative load baring supports for improved geometric X-ray CT resolution.
  • Compressive and tensile operation modes capable of imaging over 360 degrees.
  • Remote system control for in-situ X-ray CT experiments.
  • Usable for X-ray CT based experiments on the Nikon 320 kV and the High Flux Bay at the HMXIF, or the synchrotron beam lines.

Compression / Tension 5 kN Deben CT5000 Rig

Key Features

  • 10 mm linear extensometer for position readout, resolution 3 micrometer, linearity 0.1% of full scale
  • ULTEM polymer support tube for minimum X-ray attenuation (15 mm wall thickness)
  • Modular tensile and compression testing system that can be installed on the laboratory Nikon and Zeiss Versa 520 instruments at the HMXIF or synchrotron beam lines.

Tension /Compression / Torsion 10 kN Open Frame Deben Rig

Key Features

  • Specimen diameters ranging from 50 mm – 100mm.
  • Jaw spacing/travel 50-100 mm
  • Tensile or compression force capability is +/- 10 kN
  • Torsion force capability is +/- 10 Nm
  • Integrated furnace system.
  • Sample can be rotated through 360 degrees whilst maintaining tensile/compression and torsion effects
  • Rotating speeds up to 4 sec/revolution.
  • Remote system control for in-situ X-ray CT experiments.
  • Compatible with Nikon 320 kV, The High Flux Bay and synchrotron beam lines

Compression /Tension / Indentation Zeiss Xradia 810 Ultra Load Cell

Key Features

  • Specifically designed for mechanical loading (compression, tension and indentation) on the ZEISS Xradia 810 Ultra
  • Piezo actuator for closed loop displacement control with a 500 micron displacement and a resolution of 10 nanometres
  • Strain gauge force sensor with a 0.8 N maximum force and <0.1% sensitivity
  • Customizable anvil tips for different operating modes, sample types and experimental designs

Hysitron IntraSpect 360 Indentation Rig

Key Features

  • Specifically designed for in-situ XCT indentation experiments.
  • Sample diameter range: 10mm – 0.1mm and maximum sample length: 10mm.
  • Maximum applied load of 11.3 N combined with a maximum displacement of 90 microns.
  • Several available tip geometries: triangular based pyramidal Berkovich and cube-corner tips, and a 90 degree wedge diamond tip with an apex length of 100mm.
  • Compatible with ZEISS Versa 520 systems and synchrotron beamlines

650 degree Celsius MRI Furnace

Key Features

  • Temperature range from room temperature to 650 degree Celsius.
  • Specimen diameter: 0.5 mm – 15 mm.
  • Specimen length: 0.5 mm – 10 mm.
  • Capability to image specimens over 360 degrees.
  • Compatible with Nikon 320 KV, The High Flux Bay and synchrotron beamlines.

High Pressure and Temperature Fluid Flow Rig

Key Features

  • The combined systems allow pressure and temperature gradients to be generated through the sample whilst maintaining a constant confining pressure. The system can be used in the laboratory based High Flux Bay or 320kV
  • Bay or on beamlines at Diamond Light Source to image processes in situ
  • Two syringe pumps: 260ml capacity; accurate flow at pressures up to 7500 psi (500bar) and can be used with gas,water or oil based fluids.
  • Hydrothermal stirred reactor: capacity 250ml; can be pressurized up to 4500 psi (300bar) and go up to 450 °C.
  • Two imaging cells for samples with diameters up to 21mm and 5mm.
  • The cells can be used up to 220 °C and 250 bar, although it can potentially be adjusted to work at more harsh conditions.

Applications

  • Dissolution, precipitation and replacement reactions in rocks and porous materials
  • Multi-fluid flow
  • Mixing (e.g. mobilization of an oil phase trapped in a porous rock by a water based solution)
  • Dilution
  • Particle sedimentation/filtration
  • Hydrofracking and fracture healing.
National X-Ray Computed Tomography
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